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@Bruker Guides@Varian Guides
@Spectral Interpretation Workbooks

Surf these sites:
CH255 Home Page -- Excellent work. Chemical shift predictor, 1st order Multiplet maker, Spin-Spin slitting simulation, and a line shape simulation.
NMR Basics -- Getting Started with NMR. All those basic questions you were too embarrassed to ask.
NMR Instruction Archives -- NMR in Undergraduate Instruction. A few resources for teaching NMR and NMR theory.
NMR Operations for QE-300 -- Detailed directions and software commands for operating the QE-300 NMR to obtain standard proton and carbon spectra using the GE CHARM software (detailed).
NMR Sample Preparation -- How to Prepare Samples for NMR. A very good outline. Fairly accurate. You should almost always add some chemical shift reference to your sample.
NMR Samples -- And how to prepare them.
NMR Temperature Measurement -- table and references.
NMR tube requirements -- From the University of Oregon. Always use high qulity Wilmad tubes.
Resonance Reports -- A whole series of Application notes on NMR tubes, from Wilmad.
UIUC Virtual NMR Spectrometer -- A complete virtual hardware course up to acquisition

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