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Surf these sites:
 1D and 2D Experiments -- A nice little slide show on which experiment to use. Very useful.
A Guide to Structure Prediction -- (version 2)
Interpretation of NMR spectra - Exercises and Solutions -- This is a very large collection of exercises with varying degrees of difficulty in german. The solutions require a password from the author.
NMR Spectroscopy Tutorial -- With NMR problems. Good practice for the novice NMR jock.
Organic Structure Elucidation Workbook -- A set of NMR stucture determination and assignment problems, easy, moderate and hard. (Select "problems" from left frame)
University of California, Los Angeles (UCLA) -- WebSpectra
Using NMR to determine relative concentrations in a mixture -- A single interesting NMR problem. Can you guess the answer?

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